ORGNMonday, March 29, 2004

8:00 AM-12:00 PM Anaheim Convention Center -- 303A, Oral
New Reactions and Methodology
Presiding:Jon A Tunge
8:00 AM 158A facile synthesis of aryl iodides via potassium aryltrifluoroborates
George W. Kabalka, Arjun R. Mereddy
8:20 AM 159Aromatic bromination using alkyl bromides and sodium hydride in DMSO
MaoJun Guo, Fokas Demosthenes, Libing Yu, Laszlo Varady, Carmen M. Baldino
8:40 AM 160Pr(OTf)3 as an efficient and recyclable catalyst for chemoselective thioacetalization of aldehydes
Surya K De
9:00 AM 161Catalytic oxidation of sulfides to sulfones with silica gel supported ruthenium tetraoxide in non-aqueous media
Mohammed H. Ali, Lucy Thurston, Thomas P Berkbigler
9:20 AM 162Radical-mediated silyl- and germyldesulfonylation of vinyl sulfones: Synthesis of (a-fluoro)vinyl silanes and germanes
Stanislaw F. Wnuk, Pedro I. Garcia Jr., Zhizhong Wang
9:40 AM 163Synthesis of sulfonamides from activated sulfonate esters and sulfonic acids
Duncan B Judd, Caddick Stephen, Jonathan D Wilden
10:00 AM 164Synthesis of sulfones from sulfides/sulfoxides and sulfonyl chlorides from disulfides, using chlorotrimethylsilane-nitrate salt as an oxidising reagent system
G. K. Surya Prakash, Chiradeep Panja, Thomas Mathew, George A. Olah
10:20 AM 165Direct synthesis of tertiary amines in water using microwaves
Rajender Varma, Yuhong Ju
10:40 AM 166Raman spectroscopy coupled with microwave reactions
Michael J. Collins Jr., E. Keller Barnhardt
11:00 AM 167Scaling up heterogeneous microwave reactions in a flow format
Michael J. Collins Jr., Brittany L. Hayes
11:20 AM 168Microwave ring expansion reactions performed at ambient temperatures
E. Keller Barnhardt
11:40 AM 169No-D proton NMR spectroscopy as a convenient and practical method for the titration of anionic carbon (R-Li, R-MgX), nitrogen (R2N-Li), and hydride (R2Al-H, LiALH4, etc.) species
Thomas R. Hoye, Andrew W. Aspaas, Brian M. Eklov

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The 227th ACS National Meeting, Anaheim, CA, March 28-April 1, 2004