ORGNSunday, March 28, 2004

8:00 PM-10:00 PM Anaheim Convention Center -- Hall A, Poster
New Reactions and Methodology, Metal-Mediated Reactions, Heterocycles and Aromatics
Organizer:Robert D. Larsen
46A concise synthesis of (-)-cytoxazone via regioselective and stereoselective introduction of amino group using chlorosulfonyl isocyanate
Ji Duck Kim, In Soo Kim, Cheng Hua Jin, Young Hoon Jung
47Studies on the construction of vinyl-substituted adjacent quaternary centers by photochemical decarbonylation of crystalline ketones
Christopher J. Mortko, Miguel A. Garcia-Garibay
48Synthesis of enaminoketones using imidoylbenzotriazoles and silyl enol ethers
Amy E. Hayden, Kostyantyn Kirichenko
49Stereoselective preparation of b-hydroxy-b-trifluoromethyl ketones and a,b-dihydroxy-b-trifluoromethyl ketones, using chiral (L) proline as a catalyst
G. K. Surya Prakash, Chiradeep Panja, Mihirbaran Mandal, Hiriyakkanavar Ila, George A. Olah
50Ipso-Nitration of arylboronic acids: Chlorotrimethylsilane-nitrate salt as an efficient reagent system
G. K. Surya Prakash, Chiradeep Panja, Vijayalakshmi Surampudi, Nicos A. Petasis, Thomas Mathew, George A. Olah
51New exo/endo selectivity observed in monohydrolysis of dialkyl bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylates
Satomi Niwayama, Yoshikazu Hiraga
52Synthesis of substituted 3-(triisopropylsilyl)-2-naphthols
Hélène Juteau, Yves Gareau, Hugo Lachance
53Synthetic applications of vinyl tris(trimethylsilyl)silanes
Pedro I. Garcia Jr., Zhizhong Wang, Stanislaw F. Wnuk
54Synthesis and synthetic utility of pyrrole carbinols: Versatile intermediates in organic synthesis
Darren J. Dixon, Mark S. Scott
55Reaction of 1-N-SES-2,2-dimethylaziridine with aryl Grignards provides an expedient route to 2-aryl-1,1-dimethylethylamine derivatives
Leland O. Weigel, Michael B. Rice, Andrew M. Ratz
56Paper Withdrawn
57Synthesis of O-alkyl oximes
Debra D. Dolliver, David B. Delatte, Joshua Austin, James E. Johnson, Jeffrey E. Rowe, Simon G. Bott, Diana C. Canseco
58Functionalized alkenes from epoxides
David M. Hodgson, Matthew J. Fleming
59Radical cyclizations of vinylboranes with EPHP
M. Mark Midland, Diane Hinkens
60Novel uses of amino carbinols and amino alkoxides as intermediates in synthesis
Darren J. Dixon, Amanda C. Lucas
61Ynamide survivability: Studies toward the synthesis and reactivity of functional groups with ynamides
Kai-Hao Tung, Kimberly Kurtz, Richard P. Hsung
62The study of alkoxide-promoted enyne-allene cyclizations: Next generation isolated alkenes
Michelle K. Waddell, Mark A. Lipton
63Design of a new sterically hindered 1,1-dimethylallyl ester as a new protecting group for carboxylic acids
Minoo Sedighi
64Microwave-assisted amide synthesis on silica-supported carbodiimide
Shahnaz Ghassemi, Peter. C. Rahn
65Functionalization of crosslinked polystyrene nanospheres
G. K. S. Prakash, Ryan Desousa, Geroge A. Olah
66Developments of environmentally friendly organic transformations
Shui-Ling Chen, Teck-Peng Loh
67To improve the experimental system and upgrade the experimental capability
Lin-Hua Song, Cui-Yu Jiang
68Activation amines in anion-radical condensation with aromatic ketyles
Dilbar A. Turaeva, Yu V. Kurbatov
69New reagents for organic synthesis: Imidazolium dichromate/alumina as a mild and efficient heterogeneous system for cleavage of C=N
Surya K De
70DCC/DMAP-mediated coupling of carboxylic acids with oxazolidinones and thiazolidinethiones
Carlos Kleber Zago Andrade, Rafael Oliveira Rocha, Otilie Eichler Vercillo, Wender Alves Silva, Ricardo Alexandre Figueiredo Matos
71Unique microwave-assisted oxidations of carbamates and analogs utilizing an air stable dichloro-iodobenzene reagent
Walter Salamant, Christopher Hulme
72Novel LDA-mediated rearrangement of 2,2-bis(alkylsulfonyl)-1-phenylethanones: Regiospecific formation of 2-alkylsulfonylmethylsulfonyl-1-phenylethanones
Jong Kwan Bin, Jae Sang Lee, Kyongtae Kim
73Effect of solvent on the lithium - halogen exchange of primary alkyl iodides and aryl bromides
Mark R. Luderer, Jason D. Brubaker, Kevin P. Jordan, William F. Bailey
74Highly diastereoselective synthesis of (E)-1-bromo-1-trimethylgermyl-1-alkenes
Narayan G. Bhat, Noe Loredo
75Novel synthesis of (E)-gem-dimetalloalkenes containing boron and tin
Narayan G. Bhat, Nisha Varghese
76Rhodium-catalyzed [2+2+2+1] cycloaddition reaction: Application to the construction of fused 5-7-5 ring systems from various enediynes
Bibia Bennacer, Iwao Ojima
77Cp*Rh(III)-catalyzed Leuckart-Wallach-type reductive amination of ketones
Masato Kitamura, Shinji Tanaka, Tetsuya Mukai, Hajime Saburi
78Cross-metathesis reaction of vinylchlorins and vinylporphyrins
Xin Liu, Ethan Sternberg, David Dolphin
79Investigating the scope of the ring-closing metathesis reaction in the development of cyclic enol phosphonamidates
Stephen R. Sieck, Matthew D. McReynolds, Paul R. Hanson
80Simple thiazocine-2-acetic acid derivatives via ring-closing metathesis (RCM)
Dallas K. Bates, Xiaofen Li, Parag V. Jog
81Evidence for radical mechanism in olefin metathesis catalyzed by tungsten systems in a low oxidation state
Valerian Dragutan, Ileana Dragutan, Mihai Dimonie
82Radical C-C bond formation in cobalt-propargyl complexes: Stereoselective access to novel nonsteroidal hormones
Gagik G. Melikyan, Arthur Florut, Christopher Wild
83Use of the molybdenum hexacarbonyl-mediated tandem allenic Pauson-Khand reaction for the synthesis of a dicyclo[a,e]pentalene
Hui Cao, Judith L. Flippen-Anderson, Jessica L. Chen, James M. Cook
84Metal-mediated homo [6+2] cycloaddition reactions
James H. Rigby, Zeeshan Kamal, Tricia L. May, Mary J. Heeg
85One-pot, catalytic regio- and stereoselective preparation of (Z)-β-chalcogenyl acrylamides
Daniel J. Knapton, Tara Y. Meyer
86Carbonylative acetylene coupling of aryl diazonium ions with NHC-palladium catalysis
Chun Song, Yudao Ma, Merritt B. Andrus
87Highly active, air-stable combinatorial catalysts for the C-C, C-N, and C-S bond formations via cross-coupling reactions of aryl halides
George Y. Li
88Synthesis of coumestans by selective electrophilic cyclization followed by palladium-catalyzed intramolecular carbonylation: An efficient synthesis of coumestrol
Dawei Yue, Richard Larock
89Novel metal-mediated approaches for the rapid assembly of nitrogen heterocycles
Richard H. Blaauw, Sape S. Kinderman, Henk Hiemstra, Bart C.J. van Esseveldt, Floris P.J.T. Rutjes
90Ferrocene-based palladacyclic precatalysts for C-C bond forming reactions
Christopher J. Richards, Francesc X. Roca
91Palladium-mediated stereospecific synthesis of 3-enynyl substituted thioflavones/flavones via sequential Heck–Sonogashira strategy
Manojit Pal, Karuppasamy Parasuraman, Venkataraman Subramanian, Rambabu Dakarapu, Koteswar R. Yeleswarapu
92Nickel-catalyzed cross-coupling reaction of alkyl arenesulfonates with arylmagnesium bromides
Chul-Hee Cho, Tae-Yong Ryoo, Kwangyong Park
93Organocuprate oxidation with improved functional group tolerance and its application to medium ring synthesis
David S. Surry, David R. Spring
94Copper-catalyzed cross-coupling of aryl acetylenes and vinyl iodides
D. Venkataraman, Craig G. Bates, Pranorm Saejueng
95Mild and practical copper-catalyzed amination of unactivated halothiophenes
Zhikuan Lu, Robert J. Twieg
96Cu-mediated alkoxystannane addition to an allylic lactone: Application to the synthesis of sclerophytin A
Matthias C. McIntosh, Christopher M. McFarland, John M. Hutchison, Harriet A. Lindsay
97Indium-promoted additions to propargyl aldehydes: Mechanistic studies into Michael additions versus Cope rearrangements
Thomas M. Mitzel, Annie Troutman
98In-mediated b-allylation, b-propargylation, and b-allenylation onto a,b-unsaturated ketones: Reactions of in situ generated 3-tert-butyldimethylsilyloxyalk-2-enylsulfonium salts with in situ generated organoindium reagents
Phil Ho Lee, Kooyeon Lee
99Indium-promoted cross coupling reactions of acetylene moieties
Thomas M. Mitzel, Kristen M. Allegue
100Hydrogenation of 2,3-diphenylbutadiene: A revealing kinetic study
Xiuhua Cui, Kevin Burgess
101Expedient deprotection of N-Alloc group using a polymer-supported palladium catalyst in conjunction with a bound borohydride
Sukanta Bhattacharyya, Lanchi Vo, Owen W. Gooding, Jeff W. Labadie
102Steps toward the preparation of thioglycoside dendrimers
Michael J. Panigot, Angela R. Buckman, Matt Whiteside, Jeremy Lamb
103Arylation of 3-haloindoles facilitated by transient protecting group strategies
Anthony W. Thompson, Jocelyn Wang, Marzia Villa, Ryan Schoenfeld
104Novel synthesis of 5-alkyl isoquinolines
Sean C. Turner, Chih-Hung Lee, Arthur Gomtsyan, Tammie K. White
1053-Indolyl methylphosphonate and methylphosphonothioate as indicators for enzyme-based decontamination of organophosphonoate agents
Mark D. Winemiller, Fu-Lian Hsu, Fred Berg, Tu chen Cheng, Vipin K. Rastogi
106Enantioenriched 2-(metalated)-pyrrolidines
G Seelhammer
107Nucleophilic substitutions of halogenated triazoles via modifications to adjacent nitrogens
Sarah L. Poe, David R. Haines
108Rare-earth metal-catalyzed sulfonylation reactions of N-(phenylsulfonyl)pyrroles
Daniel M. Ketcha, David J. Malwitz
109DMF-DMA assisted novel Friedel-Crafts acylation of thiochroman
Yuezhong Wen, Weiping Liu
110Synthesis of multi-substituted tetrahydroquinoxalines
Xu Bai, Lianyou Zheng, Jinchang Wu
111Microwave-assisted synthesis and elaboration of fluorescein and rhodamine derivatives
Juan C. Castro, Guan-Sheng Jiao, Jin Wook Han, Kevin Burgess
112Isomer-pure synthesis of linear polycyclic aromatic heterocycles
Brigitte Wex, Bilal R. Kaafarani, Douglas C. Neckers
113Paper Withdrawn
114Synthesis of indole dimer derivatives as potential anti-tubercular drugs
Anusha Vable, Wayland E. Noland
115Design, synthesis, and biological applications of new water-soluble 4,9-diamino-3,10-perylenequinones
Xihuai Qiang, Chaobin Zheng
116Synthesis of 2-[(R-phenyl)amine]-1,4-naphthalenediones and their biological activity
Lluvia Itzel López, Elisa Leyva, Juan C. Racero
1174,8-Ditoluoyl-1,5-dihydroxynaphthalene: Efficient synthesis of multi-gram quantities
Daniel S. Tyson, Michael A. Meador
118Synthetic [2+2+2] approach to opening [60]fullerene by modification of the cage electronic structure
Shih-Ching Chuang, Saeed I. Khan, Yves Rubin
119New napelline-type diterpene alkaloid from aconitum brunneum hand-mazz
Liming Gao, Xiaomei Wei, Li Yang
120Two new diterpene alkaloids from aconitum spicatum stapf in ann
Liming Gao, Xiaomei Wei, Li Yang
121Novel synthesis of C-13 labeled pyrazinone thrombin inhibitors and elucidation of metabolic activation pathways
Jonathan Z. Ho, Matthew P. Braun, Raju Subramanian, Ying-Duo Gao, Dennis C. Dean, David G. Melillo
122Synthesis of phakellistatin 13 and conversion to phakellistatin 3 and isophakellistatin 3
David L. Van Vranken, Kevin L. Greenman, Dana M. Hach
123Development of a scalable route to a pyridoquinoxaline antiviral compound
William R. Perrault, Paul M. Herrinton, Richard A. Hohler, Joseph W. Strohbach, Steven P. Tanis, Malcolm W. Moon
124A novel cascade reaction to form indolizidine and quinolizidine alkaloids: Facile syntheses of (±)-epilupinine and (±)-tashiromine
Stephen F. Martin, Shawn M. Amorde
125Studies toward the synthesis of oxazolomycin: Stereoselective cyanosilylation of hindered cyclic ketones
Mark G Moloney, Muhammad Yaqoob
126One-pot synthesis of procaine and other pharmaceuticals
Hong Yang, Fernand C. Thyrion
127Synthesis of benzoxocane-containing natural products: Heliannuol A, K, and helianane
James R. Vyvyan, Steven T. Staben, Ryan E. Looper, Celeste Loitz
128Cyclic fluoroethers via the intramolecular cyclization of alkenyl alcohols
Melvin L. Druelinger, Daniel K. Lesniewski, Masato Yamaguchi
129Synthesis of benzofuroxans by oxidation of 2-nitroanilines and thermal and photochemical cyclization of arylazides
Mariana Salgado, Juan C. Racero, Elisa Leyva
130Synthesis of [2H,5H-dihydrofuran-3-yl]ketones
Kelsie J Betsch, Jetty Duffy-Matzner
131Intramolecular cyclization reactions of cyclic hydroxysulfone derivatives: New annulation reactions leading to oxacyclic ring systems
Aravamudan S. Gopalan, Yuan Liu, Hollie K. Jacobs
132Application of Montmorillonite clay in natural products synthesis
Matthew R. Dintzner, Kristen M. McClelland, Kara M. Morse
133Simple and convenient synthesis of coumarin-3-carboxamides
N. Srinivasa Reddy, E. Premkumar Reddy, M.V. Ramana Reddy
134Tandem intermolecular radical addition-rearrangement for azacycle synthesis
David M. Hodgson, Shuji Hachisu
135Diastereoselectivity in the aza-Cope—Mannich cyclization: Application to the synthesis of pyrrolizidine alkaloids
Harriet A. Lindsay, Maria C. Milletti, Powen Hsueh, Eun-Hoo Kim
136Practical syntheses of diazepinoindolines
Gregory S. Welmaker, Joan E. Sabalski
137Toward the synthesis of the alkaloid histrionicotoxin 285A
Helen T. Horsley, Andrew B. Holmes, Catherine J. Smith, Ian Collins
138Synthesis and biological activity of 1-ethyl-7(4-acetyl-1-piperazynil)-6-fluoroquinolone-3-carboxylic acid
Elisa Leyva, Alicia Sagredo, Angeles Cabrero, Denisse A. de Loera, Socorro Leyva
139Novel one-pot diversity oriented microwave assisted organic synthesis (MAOS) of pyrazolopyridines and tricyclic pyrazoloquinazolinones, utilizing amino-pyrazoles as a branching module
Thomas Nixey, Balan Chenera, Thomas E. Vasquez, Vijay K. Gore, Christopher Hulme
140Efficient synthesis of 3-substituted pyrimidinones
Jae Uk Jeong, Xiaohong Chen, Attiq Rahman, Dennis S. Yamashita, Juan I. Luengo
141Synthesis of 6-thiopurine analogs
Brian H. Keogh Jr., Ryan J. Rafferty, Richard M. Hyslop
142Synthesis and characterization of substituted 1,4,5,12- tetraaza-triphenylenes
Chandima Abeywickrama, A.D. Baker
143Synthesis of novel pyracyloporphyrins
Patrick J. Rauen, Timothy D. Lash
144Examination of reaction conditions for two-step, one-flask syntheses of meso-substituted corroles via dipyrromethane-dicarbinol and pyrrole
G. Richard Geier III, Jeffery Forris Beecham Chick, Jennifer B. Callinan, Christopher G. Reid, Waldemar Auguscinski
145Examination of the reaction course with different aldehydes in one-flask syntheses of meso-substituted porphyrins
Jonathan S. Lindsey, G. Richard Geier III
146Synthesis of oxynaphthiporphyrin
Jane M. Rasmussen, Timothy D. Lash
147Synthesis of dimethoxytetraarylbenziporphyrins
Joseph T. Szymanski, Timothy D. Lash
453Chiral palladium-phosphinooxazolidine catalyst for the enantioselective Diels-Alder reaction
Hiroto Nakano, Yuko Okuyama, Kouichi Takahashi, Yuichiro Suzuki, Reiko Fujita, Chizuko Kabuto

Symposium Grid -- Division of Organic Chemistry -- Session Listing

The 227th ACS National Meeting, Anaheim, CA, March 28-April 1, 2004