ORGNWednesday, March 26, 2003

9:00 AM-11:00 AM Convention Center -- Hall I-1,Poster
Heterocycles, Aromatics, Metal-Mediated Reactions, Physical Organic, Materials
Poster Session
Organizer:L. McElwee-White
482Highly diastereoselective multicomponent synthesis of unsymmetrical imidazolines
Satyamaheshwar Peddibhotla, Jetze J. Tepe
483Mechanisms of acid-catalyzed Z/E isomerization of imines in acetonitrile
James E. Johnson, Houquan Dai, Diana C. Canseco
484New approach to 1’-C-modified riboside scaffold via stereoselective functionalization of D-(+)-ribonic-g-lactone
Arnaldo H. Alzerreca
485Spectroscopic identification of carbene and carbenoid intermediates
Eric M. Tippmann, Matthew S. Platz
486Synthesis and anion-binding properties of open-chain oligopyrroles
Won-Seob Cho, Jonathan L. Sessler, Leah R. Eller, Gheorghe D. Pantos, Blake R. Peterson
487Chiral chemistry through confinement: Photocyclization of tropolone naphthalenone and cyclohexadienone derivatives included in zeolites
Lakshmi S. Kaanumalle, Ramamurthy Vaidhyanathan
488Asymmetric photoreaction in isotropic and organized media: Photochemistry of diphenylcyclopropane derivatives
Sivaguru Jayaraman, Ramamurthy Vaidhyanathan
489Enhanced enantio- and diastereoselectivity via confinement: Norrish-Yang photocyclization of a-oxoamides and 2-benzoyladamantane derivatives within zeolites
Arunkumar Natarajan, Ramamurthy Vaidhyanathan
490New blue and orange fluorescent compounds for an organic electroluminescent device
Hisato Takeuchi, Hiromitsu Tanaka, Makoto Mouri, Tomohiko Mori
491Photosensitized cyclization of alkenyl oximes
H. J. P. De Lijser, G. L. Loyo, J. R. Sawyer
492Photosensitized reactions of oximes and oxime ethers
H. J. P. De Lijser, J. R. Sawyer, C. K Tsai
493Substituent effects on photosensitized reactions of acetophenone oximes
H. J. P. De Lijser, Jason S. Kim, Suzanne M. McGrorty, Erin M. Ulloa
494Determination of self-exchange electron transfer rate constants for very fast radical cation-neutral molecule reactions
Logan K. Ausman, Jack R. Pladziewicz
495Solvothermal synthesis of polycyclic aromatic chlorocarbons carbon tetrachloride in one step
Su-Yuan Xie, Yin Peng, Meng Chen, Rong-Bin Huang, Lan-Sun Zheng
496Synthesis of 3-ethoxyindoles
Ronald W. Clawson Jr., Bjorn G.C. Soderberg
497Synthesis of 4,4’-bisphenolformal
Jiangtao Hao, David Boyles, John T. Bendler
498Synthesis of novel macrocyclic polyamine complexes for use as anticancer prodrugs
Laurie L. Parker, David J. Robins
499Synthesis of the (a,a)-5,10-bis(2-(para-fluorophynylurea)phynyl)porphyrin and anion-binding studies
Dennis H. Burns, Kenichi Calderon-Kawasaki
501Synthesis of tripyrrane analogs and related oxybenziporphyrins from resorcinol and 2-methylresorcinol
Kae Miyake, Timothy D. Lash
500Paper Withdrawn
502The quest for hydrocarbon analogs of the porphyrins
Denise A. Colby, T. D. Lash
503Superacid-catalyzed reactions of cinnamic acids and the role of superelectrophiles
Rendy Rendy, Yun Zhang, Aaron McElrea, Alma Gomez, Douglas A. Klumpp
504Synthesis and characterization of main group IV metal complexes bearing indole moieties
Taeboem Oh, Valerian Dragutan, Alex Schultz, Tania Tasu, Bernd Wrackmeyer
505Synthesis and structure of preorganized C3-symmetric trilactam scaffolds with convergently oriented thiolmethyl appendages
John E. Campbell, Steven D. Burke
506Synthesis of 2,3-diaminodihydropyrroles via a thioimidate-cyclopropane rearrangement
Christina Ng, Ronald K. Chang, Mark G. Bock, Scott D. Kuduk
507Preparation and reactions of selenium derivatives of Barton esters: A convenient route to benz[b]seleno[2,3-b]pyridines
U. Narasimha Rao, Ramadas Sathunuru, Edward R. Biehl
508Solvent and counterion effects on the NMR of disubstituted triazoliums
David R. Haines, Christine I. Worrall, Nalyn Siripong, Amanda C. Doran, Megan Chen Feetham
509Sonogashira coupling routes to fused-ring sydnones
Andrew J. Weisner, Kenneth Turnbull
510Metallation in hydrocarbon solvents: The effect of electron density localization of the directing group
R. W. Holman, Michael Timmons, Roslyn LeMastus, Phillip Shelton, Gina Jackson, B.D. Woosley, S. Brown, S. Dumbris, A. Spencer, D.W Slocum
511Mixed fused-ring oligomers as precursors to new conjugated systems
Karla R. Radke, Katsu Ogawa, Seth C. Rasmussen
512Oxidation products of a thiophene derivative and the synthesis of a novel polycyclic anhydride
Joseph W. Vincent, Robert G. Clevenger, Robert D. Ingalls, James A. Watson Jr., Douglas M. Ho, Kathleen V. Kilway
513Design and synthesis of polyhydroxy cavitands
Eric Efrain Dueno, Sandeep A. Chapalamadugu, Kirpal S. Bisht
514Dicationic electrophiles: Superacid-catalyzed chemistry of alkynes
Rendy Rendy, Yun Zhang, Aaron McElrea, Alma Gomez, Han Dang, Douglas A. Klumpp
515Direct palladium-catalyzed route for isoxazole synthesis
Matthew B. Kraft, Cindy C. Browder
516Efforts toward the total synthesis of (-)-galanthamine
Keith R. Buszek
517Facile and convenient synthesis of N-acylpyrroles from primary aromatic amides
Anil R. Ekkati, Dallas K. Bates
518A novel synthesis of 2-amino-4-(1,3-benzothiazol-2-yl)-5-(2-chloro-5-nitrophenyl)thiazole
Osvaldo Cox, Wigberto J. Hernandez, Manuel A. Ramos
519A practical preparation of 5-(ketoaryl)thiazoles
Lisa F. Frey, Karen M Marcantonio, Debra Wallace, Cheng-yi Chen, Jerry Murry, Rich D. Tillyer, Ulf H. Dolling, Edward J. J. Grabowski
520Application of the Dakin-West reaction for the synthesis of oxazole-containing dual PPAR-alpha/gamma agonists
Alexander G. Godfrey, Dawn A Brooks, James R. McCarthy, David Mitchell, Mary K. Peters, Lynne A Hay
521S-(2–Pyridinyl)-1,1,3,3-tetramethylthiouronium hexafluorophosphate: A new reagent for the synthesis of pyridine-2-thiol esters
Philip Garner, Noemi Scardovi, John D Protasiewicz
522A new Biginelli reaction procedure using potassium hydrogen sulfate as the promoter for an efficient synthesis of 3,4-dihydropyrimidin-2(1H)-one
Shujiang Tu, Fang Fang, Chunbao Miao, Hong Jiang, Daqing Shi, Xiangshan Wang
523A simple and efficient route to N-functionalized dithieno[3,2-b:2',3'-d]pyrroles: Fused-ring building blocks for new conjugated polymeric systems
Katsu Ogawa, Seth C. Rasmussen
524Lequesnamine: A new oxoaporphine alkaloid from Ocotea leucoxylon
Michael J. Imler, Mary D. Menachery, R. Rajaraman, Michael P. Cava, Alan J. Freyer, Stone. D. Shi
525Amination of 2,6-diaminopyridines with sterically demanding amines by a thermal protocol
Siegfried R. Waldvogel, Andreas Faust, Werner Barkmann
526Structure and properties of some cresolphthalein derivatives
Christopher J. Abelt, William E. Brenzovich Jr.
527Aromaticity and antiaromaticity in all-pnictogen cluster compounds: An important consequence for organic chemistry
Aleksey E. Kuznetsov, Alexander I. Boldyrev, Hua-Jin Zhai, Lai-Sheng Wang
528Synthesis of fluorescent rhodamine conjugates by reaction of primary amines with rhodamine 2'-esters
Jonathan Grote, Maciej Adamczyk
529Toward the total synthesis of selaginoidine
Michael P Cassidy, Albert Padwa
530Novel polyphenylene structures related to "cubic graphite"
Xianfeng Shen, Douglas M. Ho, Robert A. Pascal Jr.
531Synthesis of 5-amino-6-methoxy-1-(3’,4’,5’-trimethoxyphenyl)-3,4-dihydronaphthalene: A potential anticancer and vascular targeting agent
Christopher J. Jelinek, Vani Mocharla, Rogelio Siles, Zhi Chen, Kevin G. Pinney
532General synthetic approach to 2,5-disubstituted pyridines
Gregory Lannoye, Darlene Cothron
533Nitrosation reaction of phenols at basic condition with b-cyclodextrin as catalyst
Jigang Pan, Yuejun Huang
534Microwave-assisted disubstituted pyrrole synthesis
Shahnaz Ghassemi, Peter Rahn, Michael Webb
535Efficient syntheses of biologically active bicyclic oxazolino- and thiazolino[3,2-c]pyrimidin-5,7-diones
Joseph Pontillo, C. Chen
536Inhibitor-releasing quinones for reversal photography
Thomas R. Welter
537Enantiospecific synthesis of (1R,2S,4R)-4-amino-2-hydroxycyclopentanemethanol (2a) and (1S,3R)-1-aminoocyclopentanemethanol (2b)
Jonathan Z. Ho, Rafat M. Mohareb, Jin Hee Ahn, Tae Bo Sim, Henry Rapoport
538New conjugated hole transport materials for solar cells
Andrew B Holmes, Taiho Park, Niels Schulte, Saif A Haque, James Durrant, Lucy Otley, Robert J Potter, Chan Im, Heinz Baessler
539Synthesis, optical, and redox properties of alkylated 6,13-diethynylpentacenes
John E. Anthony, Christopher R. Swartz
540Donor-sigma-acceptor molecules incorporating a swallowtail perylene-bisimide acceptor
Lyle Wescott, Daniell L. Mattern
541Dynamic NMR study of organosulfur compounds: Redox-mediated molecular brake
Parag V. Jog, Richard E. Brown, Dallas K. Bates
542Energy transfer across catenane amino acids
Yoonkyung Kim, Liam C. Palmer, Csaba Nemes, Julius Rebek Jr.
543AlQ3 derivatives with tunable optical properties
Radek Pohl, Pavel Anzenbacher Jr.
544Aryl linker strategies for the synthesis of crown-ether-containing fluoropolymers
S. Clark Ligon Jr., D. W. Smith Jr., Chris M. Topping, S. Suresh, Jennifer A. Irvin, Stephen Fallis, D. D. DesMarteau
545Design and synthesis of new organometallic complexes with potential biological activity
Valerian Dragutan, Taeboem Oh, Alex Schultz, Tania Tasu, Ileana Dragutan, Mariana Danila, Petru Filip, Bernd Wrackmeyer, Larry R. Sherman
5461,2-Bis(tetrafluoropyridinylethynyl)benzenes: Synthesis and DNA photocleavage
Serguei V. Kovalenko, Igor V. Alabugin
547Novel calamitic liquid crystals: Synthesis and characterization
Kevin D. Belfield, Maher A. Qaddoura
548Photophysical and photochemical properties of a new class of photosensitizers for photodynamic therapy
Kevin D. Belfield, Claudia C. Corredor
549Chiral phase behavior in photochromic liquid crystals
Michel L. Frigoli, Georg H. Mehl
550Investigation of the photochromic properties and of the liquid-crystalline phase behavior of functionalized diarylethene derivatives
Michel L. Frigoli, Georg H. Mehl
551Optical switching and the modulation of liquid-crystal properties of functionalized diarylethene derivatives
Michel L. Frigoli, Georg H. Mehl
552Synthesis and photophysics of a T-shaped porphyrin-fullerene dyad
Ke Li, David I. Schuster
553Synthesis of a universal photolabile cross-linker and its application in AFM imaging
Rong Wang, Funing Yan, Liaohai Chen, Chada V. Gopal Reddy
554Photoregulation of hole transfer in DNA studied by a pulse radiolysis-laser flash photolysis combined method
Tadao Takada, Kiyohiko Kawai, Sachiko Tojo, Tetsuro Majima
555Photophysical characterization of thieno[3,4-b]pyrazines
Daniel J. Sattler, Kari A. Mitchell, Seth C. Rasmussen
556Substituted tris(bipyridyl)ruthenium complexes as selective photosensitizers for electron transfer in organic chemistry
Felix S. Lee, Sara Van Rooy, Norman P. Schepp
557Synthesis and characterization of a model electron donor/acceptor system based on a peptide nucleic acid duplex
Isil Dilek, Bruce A. Armitage
558Synthesis of photocleavable protecting groups for primary alcohols with applications in the construction of DNA microarrays
Garrett M. Zopp, Mary K. Boyd
559Electrocyclization reaction of N-alkylpyridones inside chirally modified zeolites
S Karthikeyan, V Ramamurthy
560Bergman cyclization: Ortho effect in benzannelated enediynes
Tarek A. Zeidan, Igor V. Alabugin
561Molecular orientation effects on hydrogen transfer rates under diffusional constraints
Michelle K. Kidder, A. C. Buchanan III, Phillip Britt
562NMR studies of the cleavage of highly substituted epoxides with organoalane reagents
José A. Prieto, Gerardo Torres
563Equilibrium lithium and cesium ion-pair acidities of some b-diketones: Aggregation of lithium and cesium ion pairs of their enolate mono- and dianions
Antonio Facchetti, Andrew Streitwieser
564Influence of methyl substituents on the stability and reactivity of 1-aza-2-adamantanone, Kirby's most twisted amide
Kathleen M. Morgan, M. Logan Rawlins, Margo Montgomery
565Conformational studies of cyanoformate (HCO2CN) and related compounds
Dalephine Davis, Diwakar Pawar, Eric Noe
566Dimethylstannylene: Generation and trapping reactions
Dong Zhou, Peter P. Gaspar
567Photochemical behavior of a-azoxy ketones
Paul S. Engel, Konstantin P. Tsvaygboym, William B. Smith
568Mechanism of dichlorocarbene addition to benzocyclopropene
Ekaterina Zelenova, Dina C. Merrer
569Dichlorocarbene addition to cyclopropenes: A computational study
Dina C. Merrer
570Mechanistic investigations of the aqueous breakdown of substituted N-(hydroxymethyl)benzamide compounds as a function of pH
Richard W. Nagorski, William J. Tenn III
571Novel regiochemistry in the aqueous singlet oxygen ene reaction of carboxylic acid salts: A comparison of substrate structure
Kristina Lynn Stensaas, Anisha Bajaj, Akram Al-Turk
572The location effect of substituents on the Bronsted apha for hydride transfer reactions
In-Sook Han Lee, Kyoung Hwha Suh
573Density functional theory investigation of deprotonation of 2,3-dihydrofuran
Zhiqing Yan, John F. Sebastian
574Cobalt-catalyzed reductive dimerization of conjugated alkenes: Application to the synthesis of macrocyclic di- and tetralactones
Chun-Chih Wang, Chien-Hong Cheng
575Novel Rh-catalyzed cyclization via rhodacycle intermediates: Hydroacylation of dienals and cycloisomerization of trienes
Yoshihiro Sato, Yoshihiro Oonishi, Miwako Mori
576Umpolung palladium- and indium-mediated allylations
John W. Giraldes, Gregory R. Cook
577New developments in palladium- and indium-mediated allylation
Gregory R. Cook, Robert Kargbo, Jason Hallman
578The contribution of prior-coordination to ortho-lithiation: Regiospecific metallation of ortho-methylanisole and dimethylbenzylamine
D.W. Slocum, Michael Timmons, Sophia Wang, Adam Watson, Carl Friesen, Dustin Smith, Roslyn LeMastus, Phillip Shelton, Gina Jackson, R. W. Holman
579Trisubstituted olefin synthesis by reaction of benzylic zinc reagents with b,b-disubstituted alkenyl(phenyl)idonium triflates
Nichole D. Litvinas, Robert J. Hinkle
580Vinyl aryl ethers from copper-catalyzed coupling of vinyl halides and phenols
Zhonghui Wan, Thomas M. Koenig, Y. John Pu, David Mitchell
581Palladium-catalyzed synthesis of isatins and 2-haloisatogens
Chet R. Howerton, Björn C. G. Söderberg, Shubhada W. Dantale
582Synthesis of 2-alkylbenzimidazoles
Jeff M. Wallace, Björn C. Söderberg
583Synthesis of indanes through coupling of ethynylstyrene derivatives with carbene complexes
Lei Zhang, James W. Herndon
584Synthesis, characterization, and elaboration of endo[n.n.n.n] (n = 3 or 4) metacyclophanes
Dennis H. Burns, Charles L. Jayne, Sumith A. Kularatne
585Rhodium-catalyzed cross-coupling of allylic alcohols with aryl- and vinylboronic acids in ionic liquids
George W Kabalka, Gang Dong, Bollu Venkataiah
586Rhodium(I)-catalyzed tandem hydrosilylation aldol reaction: Synthesis of carbocyclic natural products
Marta Freiría, William B. Motherwell, Andrew J. Whitehead
587Metalloporphyrin-based catalytic systems for olefination of aldehydes and ketones with diazo compounds
X. Peter Zhang, Ying Chen, Lingyu Huang
588Novel Rh-catalyzed [2+2+2+1] cycloaddition reaction of enediynes
Masaki Fujiwara, Victor C. Vassar, Iwao Ojima
589Palladium-catalyzed Heck-type reactions using haloalkenes in place of alkenes in reactions with organic iodides
Harold A. Dieck, Thao M. Perry, Ping Xia, Brian P. Harting
590Palladium-catalyzed cleavage of aryl propargyl ether
Manojit Pal, Karuppasamy Parasuraman, Koteswar R. Yeleswarapu
591Ligand-controlled asymmetric induction at a transition-metal-bonded stereogenic carbon: Diastereoselective synthesis of oxapalladacycles and development of their synthetic applications
Helena C. Malinakova, Janelle L. Portscheller, Sara E. Lilley
592Highly efficient Suzuki coupling reactions of aryl bromides and arylboronic acids catalyzed by Pd(OAc)2/amines under mild conditions
Bin Tao, David W. Boykin
593Indium-promoted couplings leading to enediyne formation and oxy-cope rearrangements
Thomas M. Mitzel, Annie Troutman
594Preparation of biotin derivatives by catalytic oxidative carbonylation of diamines
Yue Zhang, Kara Forinash, Lisa McElwee-White
595Synthesis of lactones and related bicyclic heterocycles by palladium(II)-catalyzed 1,4-oxidation of conjugated dienes
Renzo C. Verboom, Anders Persson, Jan-E. Bäckvall
596Toward highly air-stable palladium catalysts for the cross-coupling reactions with unactivated aryl chlorides
George Y. Li
597Isoquinolone synthesis via rhodium(II)-catalyzed intramolecular aromatic C-H insertion of a-phenylsulfonyl-a-diazoacetamides
Kyung Woon Jung, Advait S. Nagle, Cheol Hwan Yoon, Chiliu Chen
598Efficient synthesis of triols via Rh-catalyzed regioselective intramolecular silylformylation of alkynes
Bruno D. Chapsal, Chunhui Jiang, Seung-Yub Lee, Iwao Ojima
599Effect of solvent on the lithium-iodine exchange of primary alkyl iodides: Reaction of t-butyllithium with 1-iodooctane in heptane-ether mixtures
William F. Bailey, Jason D. Brubaker, Kevin P. Jordan
600A new titanium tetrachloride mediated synthesis of polysubstituted naphthalenes
George W Kabalka, Zhongzhi Wu, Yuhong Ju
601Asymmetric hydrogenation of arylalkenes using iridium imidazol-2-ylidene-oxazoline complex
Kevin Burgess, Xiuhua Cui, Marc C. Perry
602A facile reaction of (Z)-(1-bromo-1-alkenyl)boronate esters with cyclopropylmagnesium bromide: An easy access to alkyl cyclopropyl ketones
Narayan G. Bhat, Laura E. Garcia, Victoriano Tamez Jr.
603A novel synthesis of capillin and capillen via organoboranes
Narayan G. Bhat, Etem T. Chu
604An efficient and environmentally friendly synthesis of C-aryl glucals via palladium(0)-catalyzed cross-coupling reactions of triorganoindium(III) reagents and aryl halides
Thomas G Minehan, Smita Awasthi
605Palladium-catalyzed Suzuki cross-couplings of aryl chlorides in the presence of a triarylphosphine
Gregory C. Fu, Shih-Yuan Liu
606A general method for the formation of diaryl selenides using copper(I) catalysts
Rattan Gujadhur, D. Venkataraman
607Highly efficient epoxidation of cyclic alkene catalyzed by ruthenium complexes
Jian Ying Qi, C. W. Yip, Zhong Yuan Zhou, Albert S.C. Chan
608Synthesis and characterization of cobalt complexes containing 2-pyridinecarboxamide ligands and their application in catalytic oxidation of ethylbenzene with dioxygen
Jian Ying Qi, Xianjun Li, Zhong Yuan Zhou, Michael C. K. Choi, Albert S. C. Chan, Qi Yun Yang
609Synthesis of benzylic boronates via palladium-catalyzed cross-coupling reaction of bis(pinacolato)diboron with benzylic halides
Andre Giroux
610Pd-catalyzed cycloisomerization of 1,6-dienes
Guy C. Lloyd-Jones, Paul A. Slatford, I. J. S. Fairlamb, J. P. H. Charmant
611Synthesis of 7-substituted indoles via directed ortho metallation and Suzuki-Miyaura cross-coupling
Christian Hartung, Anja Fecher, Bert Nolte, Victor Snieckus

Symposium Grid -- Division of Organic Chemistry -- Session Listing

The 225th ACS National Meeting, New Orleans, LA, March 23-27, 2003